2 flow rate was 2.8 mL/min. Split ratio was 5:1. Results Twelve kinds of solvents were completely separated and determined with a good linearity (r=0.9994-0.9999).The RSD values of precision experiments and the average recovery was in line with the requirements. Conclusion Theanalytical method is simple, accurate and sensitive, which could be used for determination of residual organic solvents in Apixaban bulks drug."/>

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首頁 > 過刊瀏覽>2017年第40卷第1期 >2017,40(1):63-67. DOI:10.7501/j.issn.1674-6376.2017.01.011
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頂空氣相色譜法測定阿哌沙班原料藥中有機(jī)溶劑殘留

Determination of residual organic solvents in Apixaban bulks drug by headspace gas chromatography

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